雄甾-3,5,16-三烯-17-醇三氟甲烷磺酸酯合成路线 (共 4 条)
反应条件
in 2,6-di-tert-butyl-4-methylpyridine; dichloromethane
参考文献
British Technology Group Limited
Patent: US5604213 A1, 1997 ;
反应条件
2,6-di-tert-butyl-4-methylpyridine in dichloromethane 12 h;
参考文献
Journal of Medicinal Chemistry, , vol. 38, # 13 p. 2463 - 2471
反应条件
1: in dichloromethane 0.25 h; 2: With pyridine in dichloromethane 2 h; Product distribution / selectivity;
参考文献
WO2006/21776 A1, ;
Page/Page column 17-20 ;
反应条件
1: in ethyl acetate 0.25 h; 2: With N,N-diethylaniline in ethyl acetate 2 h; Product distribution / selectivity;
参考文献
WO2006/21776 A1, ;
Page/Page column 17-20 ;