N-苯基苯羰基亚肼酰氯合成路线 （共 129 条）
反应条件
bromine; sodium acetate; acetic acid
参考文献
Chattaway; Walker
Journal of the Chemical Society, 1925 , vol. 127, p. 983
反应条件
1: 1.) Et3N, 2.) Pb(OAc)4 / 1.) benzene, reflux, 5 h, 2.) glacial AcOH, 60 deg C, 5 min
2: 1.) H2 / 1.) 10percent Pd/C / 1.) EtOAc, 50 psi, 12 h, 2.) 150 deg C, 30 min
View Scheme
参考文献
Palazzino; Cecchi; Melani; Colotta; Filacchioni; Martini; Lucacchini
Journal of Medicinal Chemistry, 1987 , vol. 30, # 10 p. 1737 - 1742
反应条件
triethylamine in diethyl ether
1 h;
参考文献
Roesch, W.; Regitz, M.
Synthesis, 1987 , # 8 p. 689 - 693
反应条件
1: 1.) Et3N, 2.) MnO2 / 1.) benzene, 72 h, reflux; 2.) CCl4, 1 h
2: K2CO3, KMnO4 / H2O / 8 h / Heating
View Scheme
参考文献
Khlopushina, T. G.; Krinskaya, A. V.; Kirsanova, Z. D.; Zykov, D. A.; Zagorevskii, V. A.
Pharmaceutical Chemistry Journal, 1991 , vol. 25, # 11 p. 760 - 763
Khimiko-Farmatsevticheskii Zhurnal, 1991 , vol. 25, # 11 p. 10 - 13
反应条件
triethylamine in benzene
Ambient temperature;
参考文献
Wolkoff,P.; Hammerum,S.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1976 , vol. 30, p. 837 - 842
反应条件
triethylamine in benzene
10 h; Ambient temperature;
参考文献
Abbass, Ikhlass M.; Mosselhi, Mosselhi A. N.; Abdallah, Magda A.; Shawali, Ahmad S.
Journal of Chemical Research, Synopses, 1995 , # 5 p. 190 - 191
反应条件
triethylamine in benzene
24 h; Heating;
参考文献
Barzaghi, Mario; Beltrame, Pier Luigi; Dalla Croce, Piero; Del Buttero, Paola; Licandro, Emanuela; et al.
Journal of Organic Chemistry, 1983 , vol. 48, # 21 p. 3807 - 3810
反应条件
triethylamine in benzene
Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Bianchi, Giorgio; Gandolfi, Remo; Micheli, Carlo De
Journal of Chemical Research, Miniprint, 1981 , # 1 p. 135 - 158
反应条件
triethylamine
Yield given;
参考文献
Shawali, Ahmad S.; Eltawil, Bahgat A.; Albar, Hassan A.
Tetrahedron Letters, 1984 , vol. 25, # 37 p. 4139 - 4140
反应条件
triethylamine in N,N-dimethyl-formamide
3 h;
参考文献
Buzykin, B. I.; Bystrykh, N. N.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 5 p. 953 - 961
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 5 p. 1069 - 1079
