N-苯基苯羰基亚肼酰氯合成路线 (共 129 条)
反应条件
1: NEt3 / xylene / 48 h / Ambient temperature
2: BF3*OEt2 / CHCl3 / Heating
View Scheme
参考文献
Baba, N.; Soufiaoui, M.
Tetrahedron Letters, 1990 , vol. 31, # 12 p. 1709 - 1712
反应条件
bromine in tetrachloromethane
参考文献
The Upjohn Company
Patent: US4017540 A1, 1977 ;
反应条件
bromine; acetic acid
参考文献
Chattaway; Walker
Journal of the Chemical Society, 1925 , vol. 127, p. 983
参考文献
Chattaway; Walker
Journal of the Chemical Society, 1925 , vol. 127, p. 983
反应条件
1: 56 percent / dioxane / 40 h / Heating
2: 58 percent / KOH, Et3N / dimethylformamide / 10 h / Heating
View Scheme
参考文献
Buzykin, B. I.; Sysoeva, L. P.
Bull. Russ. Acad. Sci. Div. Chem. Sci. (Engl. Transl.), 1992 , vol. 41, # 6.2 p. 1424 - 1430,1115 - 1120
反应条件
triethylamine in benzene
48 h; Ambient temperature;
参考文献
Barzaghi, Mario; Beltrame, Pier Luigi; Dalla Croce, Piero; Del Buttero, Paola; Licandro, Emanuela; et al.
Journal of Organic Chemistry, 1983 , vol. 48, # 21 p. 3807 - 3810
反应条件
triethylamine in benzene
20 h; Heating;
参考文献
Barzaghi, Mario; Beltrame, Pier Luigi; Dalla Croce, Piero; Del Buttero, Paola; Licandro, Emanuela; et al.
Journal of Organic Chemistry, 1983 , vol. 48, # 21 p. 3807 - 3810
反应条件
1: 90 percent / Et3N / diethyl ether / 72 h / 20 °C / in competition reaction with 1,3-diphenyl-propynone
2: NH2OH*HCl/AcONa / ethanol / 3 h / Heating
3: 60 percent / PCl5 / diethyl ether / 48 h / Ambient temperature
View Scheme
参考文献
Bianchi, Giorgio; Gandolfi, Remo; Micheli, Carlo De
Journal of Chemical Research, Miniprint, 1981 , # 1 p. 135 - 158
反应条件
1: NEt3 / xylene / 48 h / Ambient temperature
2: BF3*OEt2 / CHCl3 / Heating
View Scheme
参考文献
Baba, N.; Soufiaoui, M.
Tetrahedron Letters, 1990 , vol. 31, # 12 p. 1709 - 1712
反应条件
triethylamine in benzene
20 h; Heating;
参考文献
Barzaghi, Mario; Beltrame, Pier Luigi; Dalla Croce, Piero; Del Buttero, Paola; Licandro, Emanuela; et al.
Journal of Organic Chemistry, 1983 , vol. 48, # 21 p. 3807 - 3810