9-(氯二甲基硅烷基)-9H-芴合成路线 (共 6 条)
反应条件
n-butyllithium 1.) ether, hexane, RT, 2 h, 2.) pentane, RT, 1 h; Yield given. Multistep reaction;
参考文献
Kukral, Juergen; Lehmus, Petri; Klinga, Martti; Leskelae, Markku; Rieger, Bernhard
European Journal of Inorganic Chemistry, 2002 , # 6 p. 1349 - 1356
反应条件
in diethyl ether; pentane T=0 - 20°C;
参考文献
Licht, Andrea I.; Schneider, Katharina J.; Alt, Helmut G.
Journal of Organometallic Chemistry, 2003 , vol. 688, # 1-2 p. 254 - 272
参考文献
Alt, Helmut G.; Jung, Michael
Journal of Organometallic Chemistry, 1998 , vol. 562, # 2 p. 229 - 253
反应条件
in hexane T=-78 - 20°C; 7 h;
参考文献
Lee, Hyosun; Lee, Choong Hoon
Journal of Organometallic Chemistry, 2004 , vol. 689, # 1 p. 214 - 223
反应条件
in tetrahydrofuran 4 h; Ambient temperature;
参考文献
Chen, You-Xian; Rausch, Marvin D.; Chien, James C. W.
Journal of Organometallic Chemistry, 1995 , vol. 497, # 1-2 p. 1 - 10
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide in diethyl ether 4 h; Title compound not separated from byproducts;
参考文献
Patsidis, Konstantinos; Alt, Helmut G.; Milius, Wolfgang; Palackal, Syriac J.
Journal of Organometallic Chemistry, 1996 , vol. 509, # 1 p. 63 - 71