5-(二甲氨基)甲基-2-呋喃甲醇合成路线 （共 16 条）
反应条件
sodium carbonate in tetrahydrofuran; hydrogenchloride
参考文献
Glaxo Group Limited
Patent: US4394516 A1, 1983 ;
参考文献
Allen and Hanburys Limited
Patent: US4128658 A1, 1978 ;
参考文献
Bristol-Myers Company
Patent: US4510309 A1, 1985 ;
US 4510309 A
反应条件
hydrogenchloride; thiourea
1.) 65 - 70 deg C, 4.5 h, 2.) room temp., 22 h;
参考文献
Sorba; Fruttero; Calvino; Gasco; Orsetti
Archiv der Pharmazie, 1984 , vol. 317, # 6 p. 496 - 501
反应条件
1: 75 percent / thiourea, 6 N HCl / 1.) 65 - 70 deg C, 4.5 h, 2.) room temp., 22 h
2: 74 percent / sodium ethoxide / ethanol
View Scheme
参考文献
Sorba; Fruttero; Calvino; Gasco; Orsetti
Archiv der Pharmazie, 1984 , vol. 317, # 6 p. 496 - 501
参考文献
Tsuboyama; Yanagita
Scientific Papers of the Institute of Physical and Chemical Research (Japan), 1959 , vol. 53, p. 318,327
