2-氯-5,8-二甲氧基-3-喹啉甲醛合成路线 (共 3 条)
反应条件
trichlorophosphate in N-methyl-acetamide
参考文献
American Cyanamid Company
Patent: US5026859 A1, 1991 ;
反应条件
trichlorophosphate T=85°C; 24 h;
参考文献
Fernandez-Galleguillos, Carlos; Saavedra, Luis A.; Gutierrez, Margarita
Journal of the Brazilian Chemical Society, 2014 , vol. 25, # 2 p. 365 - 371
反应条件
1.1: triethylamine / chloroform / 1 h / 0 °C 2.1: trichlorophosphate / 0 - 75 °C / Inert atmosphere 2.2: 0.5 h / 0 - 10 °C / Inert atmosphere View Scheme
参考文献
Fernandez-Galleguillos, Carlos; Saavedra, Luis A.; Gutierrez, Margarita
Journal of the Brazilian Chemical Society, 2014 , vol. 25, # 2 p. 365 - 371