您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
154344-24-8
合成路线
（共 3 条）
154344-24-8
→
反应条件
3445-78-1
反应条件
tetraphosphorus decasulfide in xylene 2 h; Heating;
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
154344-24-8
→
反应条件
65282-42-0
反应条件
1: I2; NaHCO3 / ethanol 2: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 3: H2S / ethanol / pH 7.4 4: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 5: ethanol / Heating 6: I2; NaHCO3 / ethanol 7: Lawesson's reagent / toluene / 0.5 h / Heating 8: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 9: H2S / ethanol / pH 7.4 10: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 11: ethanol / Heating 12: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 13: ethanol / Heating 14: I2; NaHCO3 / ethanol 15: Lawesson's reagent / toluene / 0.5 h / Heating 16: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 17: H2S / ethanol / pH 7.4 18: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 19: ethanol / Heating 20: I2; NaHCO3 / ethanol 21: Lawesson's reagent / toluene / 0.5 h / Heating 22: H2S / ethanol / pH 7.4 23: I2; NaHCO3 / ethanol 24: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 25: H2S / ethanol / pH 7.4 26: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 27: ethanol / Heating 28: I2; NaHCO3 / ethanol 29: Lawesson's reagent / toluene / 0.5 h / Heating 30: H2S / ethanol / pH 7.4 31: I2; NaHCO3 / ethanol 32: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 33: H2S / ethanol / pH 7.4 34: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
154344-24-8
→
反应条件
91859-66-4
反应条件
1: I2; NaHCO3 / ethanol 2: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 3: H2S / ethanol / pH 7.4 4: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 5: ethanol / Heating 6: I2; NaHCO3 / ethanol 7: Lawesson's reagent / toluene / 0.5 h / Heating 8: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 9: H2S / ethanol / pH 7.4 10: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 11: ethanol / Heating 12: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 13: ethanol / Heating 14: I2; NaHCO3 / ethanol 15: Lawesson's reagent / toluene / 0.5 h / Heating 16: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
