反应条件
1: H2S / ethanol / pH 7.4 2: I2; NaHCO3 / ethanol 3: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 4: H2S / ethanol / pH 7.4 5: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 6: ethanol / Heating 7: I2; NaHCO3 / ethanol 8: Lawesson's reagent / toluene / 0.5 h / Heating 9: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 10: H2S / ethanol / pH 7.4 11: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 12: ethanol / Heating 13: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 14: ethanol / Heating 15: I2; NaHCO3 / ethanol 16: Lawesson's reagent / toluene / 0.5 h / Heating 17: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 18: H2S / ethanol / pH 7.4 19: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 20: ethanol / Heating 21: I2; NaHCO3 / ethanol 22: Lawesson's reagent / toluene / 0.5 h / Heating 23: H2S / ethanol / pH 7.4 24: I2; NaHCO3 / ethanol 25: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 26: H2S / ethanol / pH 7.4 27: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 28: ethanol / Heating 29: I2; NaHCO3 / ethanol 30: Lawesson's reagent / toluene / 0.5 h / Heating 31: H2S / ethanol / pH 7.4 32: I2; NaHCO3 / ethanol 33: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 34: H2S / ethanol / pH 7.4 35: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 36: 77 percent / Lawesson's reagent / toluene / 3 h / Heating 37: ethanol / Heating 38: P4S10 / xylene / 2 h / Heating 39: ethanol / Heating 40: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 41: I2; NaHCO3 / ethanol 42: Lawesson's reagent / toluene / 0.5 h / Heating 43: H2S / ethanol / pH 7.4 44: P4S10 / xylene / 2 h / Heating 45: ethanol / Heating 46: P4S10 / xylene / 2 h / Heating View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
