反应条件
1: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 2: H2S / ethanol / pH 7.4 3: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 4: ethanol / Heating 5: I2; NaHCO3 / ethanol 6: Lawesson's reagent / toluene / 0.5 h / Heating 7: H2S / ethanol / pH 7.4 8: I2; NaHCO3 / ethanol 9: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 10: H2S / ethanol / pH 7.4 11: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 12: ethanol / Heating 13: I2; NaHCO3 / ethanol 14: Lawesson's reagent / toluene / 0.5 h / Heating 15: H2S / ethanol / pH 7.4 16: I2; NaHCO3 / ethanol 17: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 18: H2S / ethanol / pH 7.4 19: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 20: 77 percent / Lawesson's reagent / toluene / 3 h / Heating 21: ethanol / Heating 22: P4S10 / xylene / 2 h / Heating 23: ethanol / Heating 24: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 25: I2; NaHCO3 / ethanol 26: Lawesson's reagent / toluene / 0.5 h / Heating 27: H2S / ethanol / pH 7.4 28: P4S10 / xylene / 2 h / Heating 29: ethanol / Heating 30: P4S10 / xylene / 2 h / Heating 31: ethanol / Heating 32: P4S10 / xylene / 2 h / Heating 33: ethanol / Heating 34: I2; NaHCO3 / ethanol 35: H2S / ethanol / pH 7.4 36: P4S10 / xylene / 2 h / Heating 37: ethanol / Heating 38: P4S10 / xylene / 2 h / Heating View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
