反应条件
1: Lawesson's reagent / toluene / 0.5 h / Heating 2: H2S / ethanol / pH 7.4 3: I2; NaHCO3 / ethanol 4: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 5: H2S / ethanol / pH 7.4 6: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 7: ethanol / Heating 8: I2; NaHCO3 / ethanol 9: Lawesson's reagent / toluene / 0.5 h / Heating 10: H2S / ethanol / pH 7.4 11: I2; NaHCO3 / ethanol 12: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 13: H2S / ethanol / pH 7.4 14: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 15: 77 percent / Lawesson's reagent / toluene / 3 h / Heating 16: ethanol / Heating 17: P4S10 / xylene / 2 h / Heating 18: ethanol / Heating 19: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 20: I2; NaHCO3 / ethanol 21: Lawesson's reagent / toluene / 0.5 h / Heating 22: H2S / ethanol / pH 7.4 23: P4S10 / xylene / 2 h / Heating 24: ethanol / Heating 25: P4S10 / xylene / 2 h / Heating 26: ethanol / Heating 27: P4S10 / xylene / 2 h / Heating 28: ethanol / Heating 29: I2; NaHCO3 / ethanol 30: H2S / ethanol / pH 7.4 31: P4S10 / xylene / 2 h / Heating 32: ethanol / Heating 33: P4S10 / xylene / 2 h / Heating View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
