反应条件
1: Lawesson's reagent / toluene / 0.5 h / Heating 2: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 3: H2S / ethanol / pH 7.4 4: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 5: ethanol / Heating 6: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 7: ethanol / Heating 8: I2; NaHCO3 / ethanol 9: Lawesson's reagent / toluene / 0.5 h / Heating 10: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 11: H2S / ethanol / pH 7.4 12: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 13: ethanol / Heating 14: I2; NaHCO3 / ethanol 15: Lawesson's reagent / toluene / 0.5 h / Heating 16: H2S / ethanol / pH 7.4 17: I2; NaHCO3 / ethanol 18: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 19: H2S / ethanol / pH 7.4 20: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 21: ethanol / Heating 22: I2; NaHCO3 / ethanol 23: Lawesson's reagent / toluene / 0.5 h / Heating 24: H2S / ethanol / pH 7.4 25: I2; NaHCO3 / ethanol 26: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 27: H2S / ethanol / pH 7.4 28: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 29: 77 percent / Lawesson's reagent / toluene / 3 h / Heating 30: ethanol / Heating 31: P4S10 / xylene / 2 h / Heating 32: ethanol / Heating 33: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 34: I2; NaHCO3 / ethanol 35: Lawesson's reagent / toluene / 0.5 h / Heating 36: H2S / ethanol / pH 7.4 37: P4S10 / xylene / 2 h / Heating 38: ethanol / Heating 39: P4S10 / xylene / 2 h / Heating View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
