反应条件
1: Lawesson's reagent / toluene / 0.5 h / Heating 2: H2S / ethanol / pH 7.4 3: I2; NaHCO3 / ethanol 4: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 5: H2S / ethanol / pH 7.4 6: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 7: 77 percent / Lawesson's reagent / toluene / 3 h / Heating 8: ethanol / Heating 9: P4S10 / xylene / 2 h / Heating 10: ethanol / Heating 11: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 12: I2; NaHCO3 / ethanol 13: Lawesson's reagent / toluene / 0.5 h / Heating 14: H2S / ethanol / pH 7.4 15: P4S10 / xylene / 2 h / Heating 16: ethanol / Heating 17: P4S10 / xylene / 2 h / Heating 18: ethanol / Heating 19: P4S10 / xylene / 2 h / Heating 20: ethanol / Heating 21: I2; NaHCO3 / ethanol 22: H2S / ethanol / pH 7.4 23: P4S10 / xylene / 2 h / Heating 24: ethanol / Heating 25: P4S10 / xylene / 2 h / Heating View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
