反应条件
1: H2S / ethanol / pH 7.4 2: I2; NaHCO3 / ethanol 3: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 4: H2S / ethanol / pH 7.4 5: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 6: ethanol / Heating 7: I2; NaHCO3 / ethanol 8: Lawesson's reagent / toluene / 0.5 h / Heating 9: H2S / ethanol / pH 7.4 10: I2; NaHCO3 / ethanol 11: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 12: H2S / ethanol / pH 7.4 13: 90 percent / Lawesson's reagent / toluene / 0.5 h / Heating 14: 77 percent / Lawesson's reagent / toluene / 3 h / Heating 15: ethanol / Heating 16: P4S10 / xylene / 2 h / Heating 17: ethanol / Heating 18: Hg(OAc)2; AcOH / CHCl3 / 0.5 h / 20 °C 19: I2; NaHCO3 / ethanol 20: Lawesson's reagent / toluene / 0.5 h / Heating 21: H2S / ethanol / pH 7.4 22: P4S10 / xylene / 2 h / Heating 23: ethanol / Heating 24: P4S10 / xylene / 2 h / Heating 25: ethanol / Heating 26: P4S10 / xylene / 2 h / Heating 27: ethanol / Heating 28: I2; NaHCO3 / ethanol 29: H2S / ethanol / pH 7.4 30: P4S10 / xylene / 2 h / Heating 31: ethanol / Heating 32: P4S10 / xylene / 2 h / Heating View Scheme
参考文献
Pregnolato, Massimo; Terreni, Marco; Ubiali, Daniela; Pagani, Giuseppe; Borgna, Pietro; Pastoni, Fiorenzo; Zampollo, Fabrizio
Farmaco, 2000 , vol. 55, # 11-12 p. 669 - 679
