7,8-二氢-1H,6H-喹啉-2,5-二酮合成路线 （共 19 条）
反应条件
T=170°C; Neat (no solvent);
参考文献
Stachel, Shawn J.; Steele, Thomas G.; Petrocchi, Alessia; Haugabook, Sharie J.; McGaughey, Georgia; Katharine Holloway; Allison, Timothy; Munshi, Sanjeev; Zuck, Paul; Colussi, Dennis; Tugasheva, Katherine; Wolfe, Abigail; Graham, Samuel L.; Vacca, Joseph P.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 1 p. 240 - 244
反应条件
1: 27 percent / ethanol / 2 h / Heating 2: 72 percent / diphenyl ether / 0.5 h / Heating View Scheme
参考文献
Heterocycles, , vol. 34, # 5 p. 991 - 1004
反应条件
1: 73 percent / 10percent HCl / 2 h / Heating 2: 86 percent / ammonium acetate, glacial acetic acid / 1 h / Heating View Scheme
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 27, # 1 p. 71 - 76
Khimiya Geterotsiklicheskikh Soedinenii, , # 1 p. 86 - 92
反应条件
1: 80 percent / Ag2CO3 / toluene / 48 h 2: 95 percent / pyridine / 16 h / 20 °C 3: 29 percent / BH3*THF / 12 h / 20 °C View Scheme
参考文献
Carlier, Paul R.; Du, Da-Ming; Han, Yi-Fan; Liu, Jing; Perola, Emanuele; Williams, Ian D.; Pang, Yuan-Ping
Angewandte Chemie (International Edition in English), 2000 , vol. 39, # 10 p. X1775-1777
反应条件
palladium on activated charcoal in decalin 144 h; Heating;
参考文献
Fernandez, Maria; Cuesta, Elena de la; Avendano, Carmen
Heterocycles, 1994 , vol. 38, # 12 p. 2615 - 2620
反应条件
trichlorophosphate in acetonitrile T=75°C; 1.25 h; Inert atmosphere;
参考文献
US2014/31391 A1, ;
Paragraph 0368; 0369; 0370 ;
反应条件
sodium methylate in tetrahydrofuran
参考文献
Carlier, Paul R.; Han, Yifan; Pang, Yuan-Ping; Du, Da-Ming
Patent: US2002/156096 A1, 2002 ;
参考文献
Carlier, Paul R.; Han, Yifan; Pang, Yuan-Ping; Du, Da-Ming
Patent: US2002/156096 A1, 2002 ;
反应条件
silver carbonate in chloroform
T=20°C; Alkylation; 48 h;
参考文献
Carlier, Paul R.; Du, Da-Ming; Han, Yi-Fan; Liu, Jing; Perola, Emanuele; Williams, Ian D.; Pang, Yuan-Ping
Angewandte Chemie (International Edition in English), 2000 , vol. 39, # 10 p. X1775-1777
