3-二甲基氨基-2,2-二甲基丙醛合成路线 （共 11 条）
参考文献
Sato, Masakazu; Kakinuma, Hiroyuki; Amada, Hideaki
Patent: US2006/4078 A1, 2006 ;
Location in patent: Page/Page column 5 ;
参考文献
Mannich; Wieder
Chemische Berichte, 1932 , vol. 65, p. 385,389
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Mannich
Patent: HU101428 ;
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Mannich
Patent: US1824676 , 1930 ;
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Lesser,B.
Diss. <Frankfurt/M. 1930> S. 12
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Mannich
Patent: DE542253 , 1928 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 2986,2987
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Mannich
Patent: DE544692 , 1930 ;
参考文献
Kinast,G.; Tietze,L.-F.
Angewandte Chemie, 1976 , vol. 88, p. 261 - 262
参考文献
Brannock,K.C. et al.
Journal of Organic Chemistry, 1964 , vol. 29, p. 2579 - 2582
反应条件
trifluoroacetic acid 1) CH3CN, 30 min, room temperature, 2) 21 h, room temperature; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Griengl, Herfried; Prischl, Gerhard; Bleikolm, Anton
Liebigs Annalen der Chemie, 1980 , # 10 p. 1573 - 1582
反应条件
trifluoroacetic acid 1) THF, 30 min, room temperature, 2) 40 h, room temperature; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Griengl, Herfried; Prischl, Gerhard; Bleikolm, Anton
Liebigs Annalen der Chemie, 1980 , # 10 p. 1573 - 1582
反应条件
trifluoroacetic acid 1) THF, 30 min, room temperature, 2) 40 h, room temperature; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Griengl, Herfried; Prischl, Gerhard; Bleikolm, Anton
Liebigs Annalen der Chemie, 1980 , # 10 p. 1573 - 1582
反应条件
methanol; nickel T=70 - 90°C; durch reduktive Aminierung;
参考文献
Hoffmann-La Roche A.G.
Patent: DE572548 , 1932 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 19, p. 1505
参考文献
Anderson,A.G.; Wills,M.T.
Journal of Organic Chemistry, 1968 , vol. 33, # 2 p. 536 - 541
反应条件
methanol; platinum Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 61, p. 1200,1201
