4-(N-苯甲酰基氨基)苯酚合成路线 (共 39 条)
反应条件
in various solvent(s)
T=15°C; 0.333333 h;
参考文献
Ueda, Mitsuru; Seki, Kouji; Imai, Yoshio
Synthesis, 1981 , # 12 p. 991 - 993
反应条件
in tetrahydrofuran
T=18°C; 12 h;
参考文献
Kang, Young-Jin; Chung, Hyun-A; Kim, Jeum-Jong; Yoon, Yong-Jin
Synthesis, 2002 , # 6 p. 733 - 738
反应条件
potassium tert-butylate in tetrahydrofuran
T=20°C;
参考文献
Mashraqui, Sabir Hussain; Shivaji, Jadhav Latika
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 5 p. 927 - 935
反应条件
iodine in acetonitrile
Beckmann rearrangement; 5 h; Reflux;
参考文献
Ganguly, Nemai C.; Mondal, Pallab
Synthesis, 2010 , # 21 art. no. Z16110SS, p. 3705 - 3709
反应条件
tetrachloromethane; tributylphosphine in acetonitrile
115 h; Ambient temperature;
参考文献
Kikugawa, Yasuo; Mitsui, Kimiyo
Chemistry Letters, 1993 , # 8 p. 1369 - 1372
反应条件
in N,N-dimethyl-formamide
T=70 - 80°C; 4 h;
参考文献
Mashraqui, Sabir H.; Shivaji, Jadhav L.
Journal of Chemical Research - Part S, 2003 , # 3 p. 121 - 123
反应条件
in N,N-dimethyl-formamide
T=80 - 90°C; 4 h;
参考文献
Mashraqui, Sabir Hussain; Shivaji, Jadhav Latika
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 5 p. 927 - 935
反应条件
1-methyl-pyrrolidin-2-one; potassium carbonate; thiophenol
2 h; Heating;
参考文献
Chakraborti, Asit K.; Sharma, Lalima; Nayak, Mrinal K.
Journal of Organic Chemistry, 2002 , vol. 67, # 18 p. 6406 - 6414
反应条件
1.1: 87 percent / thionyl chloride / 0 - 20 °C
2.1: n-butyl lithium / hexane; tetrahydrofuran / 1 h / 20 °C
2.2: 62 percent / hexane; tetrahydrofuran / 12 h / 20 °C
View Scheme
参考文献
Faler, Catherine A.; Joullie, Madeleine M.
Tetrahedron Letters, 2006 , vol. 47, # 40 p. 7229 - 7231
反应条件
SnCl2·2H2O; tetra-(n-butyl)ammonium iodide in acetonitrile
Beckmann Rearrangement; 0.75 h; Molecular sieveReflux;
参考文献
Ganguly, Nemai C.; Nayek, Subhasis; Chandra, Sumanta
Journal of the Indian Chemical Society, 2013 , vol. 90, # 10 p. 1695 - 1702