反应条件
1: 1.) (1R,2S)-N-pyrrolidinylnorephedrine lithium alkoxide, triphenylmethane / 1.) THF, toluene, hexanes, 0-5 deg C, 30 min, 2.) THF, toluene, hexanes, -55 deg C, 60 min 2: 91 percent / triethylamine / toluene / 1 h 3: 76 percent / ceric ammonium nitrate / acetonitrile; H2O / 1 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 63, # 23 p. 8536 - 8543