反应条件
1: 77 percent / Amberlyst-15 / methanol / 6 h / 45 °C
2: 1.) (COCl)2, DMSO, 2.) Et3N / 1.) CH2Cl2, -60 deg C, 15 min, 2.) CH2Cl2, -60 deg C, 5 min
3: AgNO3, aq. NaOH / 0.08 h / 0 °C
View Scheme
参考文献
Dado; Gellman
Journal of the American Chemical Society, 1994 , vol. 116, # 3 p. 1054 - 1062
