(S)-N-叔丁氧羰基-alpha-(碘甲基)苯乙胺合成路线 （共 6 条）
反应条件
1H-imidazole; diphenylphosphinopolystyrene; iodine in dichloromethane 1 h; Heating;
参考文献
Bolognese, Adele; Fierro, Olga; Guarino, Daniela; Longobardo, Luigi; Caputo, Romualdo
European Journal of Organic Chemistry, 2006 , # 1 p. 169 - 173
反应条件
sodium iodide in acetone T=20°C; 24 h;
参考文献
Ohno; Anzai; Toda; Ohishi; Fujii; Tanaka; Takemoto; Ibuka
Journal of Organic Chemistry, 2001 , vol. 66, # 14 p. 4904 - 4914
反应条件
1: 88 percent / CHCl3 / 0 - 20 °C 2: 86 percent / iodine; triphenylphosphine polystyryl-supported; imidazole / CH2Cl2 / 2 h / Heating View Scheme
参考文献
Hunter, Christopher; Jackson, Richard F. W.; Rami, Harshad K.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 2 p. 219 - 223
反应条件
1: 90 percent / triethylamine / tetrahydrofuran / 2 h 2: 92 percent / polystyryl diphenylphosphine, imidazole, iodine / CH2Cl2 / 1 h / Heating View Scheme
参考文献
Hunter, Christopher; Jackson, Richard F. W.; Rami, Harshad K.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 2 p. 219 - 223
反应条件
1: 97 percent / lithium borohydride; trimethylsilyl chloride / tetrahydrofuran / 0.25 h / 20 °C 2: 88 percent / CHCl3 / 0 - 20 °C 3: 86 percent / iodine; triphenylphosphine polystyryl-supported; imidazole / CH2Cl2 / 2 h / Heating View Scheme
参考文献
Quagliato, Dominick A.; Andrae, Patrick M.; Matelan, Edward M.
Journal of Organic Chemistry, 2000 , vol. 65, # 16 p. 5037 - 5042
反应条件
in dichloromethane 4 h; Heating;
参考文献
Tetrahedron, , vol. 51, # 45 p. 12337 - 12350
