2-((叔丁基二苯基甲硅烷基)氧基)-N-甲氧基-N-甲基乙酰胺合成路线 （共 4 条）
反应条件
dicyclohexyl-carbodiimide in dichloromethane Reflux;
参考文献
Ascenso, Osvaldo S.; Marques, Joao C.; Santos, Ana Rita; Xavier, Karina B.; Rita Ventura; Maycock, Christopher D.
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 3 p. 1236 - 1241
反应条件
trimethylaluminum in hexane; dichloromethane 1.) -15 deg C, 30 min; room temp., 35 min, 2.) room temp., 2 h;
参考文献
Nemoto, Hideo; Nagamochi, Masatoshi; Ishibashi, Hiroki; Fukumoto, Keiichiro
Journal of Organic Chemistry, 1994 , vol. 59, # 1 p. 74 - 79
反应条件
1: 100 percent / imidazole, DMAP / dimethylformamide / 10 h / Ambient temperature 2: 97 percent / Me3Al / CH2Cl2; hexane / 1.) -15 deg C, 30 min; room temp., 35 min, 2.) room temp., 2 h View Scheme
参考文献
Ascenso, Osvaldo S.; Marques, Joao C.; Santos, Ana Rita; Xavier, Karina B.; Rita Ventura; Maycock, Christopher D.
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 3 p. 1236 - 1241
反应条件
1: water; lithium hydroxide hydrate / tetrahydrofuran / 20 °C 2: dicyclohexyl-carbodiimide / dichloromethane / Reflux View Scheme
参考文献
Ascenso, Osvaldo S.; Marques, Joao C.; Santos, Ana Rita; Xavier, Karina B.; Rita Ventura; Maycock, Christopher D.
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 3 p. 1236 - 1241
