1-叠氮基-2-(三氟甲基)苯合成路线 (共 3 条)
反应条件
1: With hydrogenchloride; sodium nitrite in water 0.0833333 h; Cooling with ice; 2: With sodium azide in water T=20°C; 1.08333 h; Cooling with ice;
参考文献
LIFE and BRAIN GMBH; MUeLLER, Christa; ZIMMER, Andreas; LABS, Stefanie; BUCHHOLZ, Stephanie; HINZ, Sonja
Patent: WO2012/76974 A1, 2012 ;
Location in patent: Page/Page column 36-37 ;
反应条件
potassium hydroxide; hydrogen fluoride in hexane; dichloromethane; water
反应条件
in tetrahydrofuran; methanol 15 h; Irradiation;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 2 p. 249 - 254