N,N-二甲基苯硫代甲酰胺合成路线 （共 49 条）
反应条件
thiophosphorylated amine resin in toluene T=90°C; 30 h;
参考文献
Cho, Dongho; Ahn, Jiyoung; De Castro, Kathlia A.; Ahn, Hyunseok; Rhee, Hakjune
Tetrahedron, 2010 , vol. 66, # 30 p. 5583 - 5588
反应条件
sulfur; sodium acetate in N,N-dimethyl-formamide T=100°C; 3 h;
参考文献
Amupitan, Joseph O.
Synthesis, 1983 , # 9 p. 730
反应条件
Lawesson's reagent in toluene 5 h; Inert atmosphereReflux;
参考文献
Hori, Tetsuharu; Otani, Yuko; Kawahata, Masatoshi; Yamaguchi, Kentaro; Ohwada, Tomohiko
Journal of Organic Chemistry, 2008 , vol. 73, # 22 p. 9102 - 9108
反应条件
triethylamine in acetonitrile T=20°C; Cyclization; elimination; dealkylation; 2 h;
参考文献
Magedov; Przheval'skii; Yufit; Droza
Russian Chemical Bulletin, 1997 , vol. 46, # 4 p. 759 - 763
反应条件
bis(trimethylsilyl)-sulfide in tetrahydrofuran Heating;
参考文献
Mizhiritskii, M. D.; Reikhsfel'd, V. O.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 7 p. 1547 - 1558,1373 - 1382
反应条件
sulfur; copper acetylacetonate; potassium carbonate T=110°C; 24 h; Schlenk technique; Reagent/catalystSolvent;
参考文献
Qu, Yanyang; Li, Zhengkai; Xiang, Haifeng; Zhou, Xiangge
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 16 p. 3141 - 3146
反应条件
in tetrachloromethane T=40 - 50°C; 5 h;
参考文献
Mizhiritskii, M. D.; Reikhsfel'd, V. O.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 7 p. 1547 - 1558,1373 - 1382
反应条件
hydrogen sulfide in dichloromethane
参考文献
Smith, D. C.; Lee, S. W.; Fuchs, P. L.
Journal of Organic Chemistry, 1994 , vol. 59, # 2 p. 348 - 354
反应条件
sulfur; copper acetylacetonate; pentanal; potassium carbonate T=110°C; 24 h; Schlenk technique;
参考文献
Qu, Yanyang; Li, Zhengkai; Xiang, Haifeng; Zhou, Xiangge
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 16 p. 3141 - 3146
参考文献
Schroth, Werner; Andersch, Joerg
Synthesis, 1989 , # 3 p. 202 - 204
