N,N-二甲基苯硫代甲酰胺合成路线 （共 49 条）
反应条件
pyridine; tetraphosphorus decasulfide 1) reflux, 0.5 h, 2) pyridine, reflux, 2 h; Multistep reaction;
参考文献
Silva, Maria D. M. C. Ribeiro da; Souza, Pilar; Pilcher, Geoffrey
Journal of Chemical Thermodynamics, 1989 , vol. 21, # 2 p. 173 - 178
参考文献
Brown,J.P.; Thompson,M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1974 , p. 863 - 866
参考文献
Perregaard,J. et al.
Bulletin des Societes Chimiques Belges, 1977 , vol. 86, p. 321 - 328
参考文献
Perregaard,J. et al.
Bulletin des Societes Chimiques Belges, 1977 , vol. 86, p. 321 - 328
参考文献
Huisgen,R. et al.
Justus Liebigs Annalen der Chemie, 1962 , vol. 658, p. 169 - 180
反应条件
benzo[1,3,2]dioxaborole 1.) CH2Cl2, reflux, 6 h, 2.) 20 deg C, 15 h; Yield given. Multistep reaction;
参考文献
Jabre, Imad; Saquet, Monique; Truillier, Andre
Journal of Chemical Research, Miniprint, 1990 , # 4 p. 756 - 784
反应条件
hydrogen sulfide 1.) CH2Cl2, THF, 18 deg C, 50 h, 2.) pyridine, 5 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Beale, Michael H.; Gaskin, Paul; Kirkwood, Paul S.; MacMillan, Jake
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 885 - 891
反应条件
pyridine; hydrogen sulfide; N-ethyl-N,N-diisopropylamine 1.) dichloromethane, room temperature, 44 h, 2.) 5 min; Yield given. Multistep reaction;
参考文献
Kirkwood, Paul S.; MacMillan, Jake
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 689 - 698
反应条件
pyridine; ent-1α,13-diacetoxy-3α,10-dihydroxy-20-norgibberell-16-ene-7,19-dioic acid 7-methyl ester 19,10-lactone; hydrogen sulfide; N-ethyl-N,N-diisopropylamine 1.) dichloromethane, room temperature, 64 h; 2.) 5 min; Yield given. Multistep reaction;
参考文献
Kirkwood, Paul S.; MacMillan, Jake
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 689 - 698
反应条件
benzo[1,3,2]dioxaborole 1.) CH2Cl2, 0 deg C, 30 min, 2.) 20 deg C, 15 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Jabre, Imad; Saquet, Monique; Truillier, Andre
Journal of Chemical Research, Miniprint, 1990 , # 4 p. 756 - 784
