4-[4-(甲烷磺酰基氧基)-1-丁炔基]-alpha,alpha-二(甲基)苯乙酸,甲酯合成路线 （共 4 条）
反应条件
1: 75 percent / K2CO3 / acetonitrile / 12 h / Heating 2: 75 percent / HgO, aq. H2SO4 / methanol / 3 h / 55 °C 3: 95 percent / NaBH4 / methanol / 20 h / Ambient temperature 4: 76 percent / aq. KOH / methanol / 16 h / 80 °C View Scheme
参考文献
Kawai, Stephen H.; Hambalek, Robert J.; Just, George
Journal of Organic Chemistry, 1994 , vol. 59, # 9 p. 2620 - 2622
反应条件
potassium carbonate in acetonitrile 12 h; Heating;
参考文献
Kawai, Stephen H.; Hambalek, Robert J.; Just, George
Journal of Organic Chemistry, 1994 , vol. 59, # 9 p. 2620 - 2622
反应条件
1: 75 percent / K2CO3 / acetonitrile / 12 h / Heating 2: 75 percent / HgO, aq. H2SO4 / methanol / 3 h / 55 °C View Scheme
参考文献
Kawai, Stephen H.; Hambalek, Robert J.; Just, George
Journal of Organic Chemistry, 1994 , vol. 59, # 9 p. 2620 - 2622
反应条件
1: 75 percent / K2CO3 / acetonitrile / 12 h / Heating 2: 75 percent / HgO, aq. H2SO4 / methanol / 3 h / 55 °C 3: 95 percent / NaBH4 / methanol / 20 h / Ambient temperature View Scheme
参考文献
Kawai, Stephen H.; Hambalek, Robert J.; Just, George
Journal of Organic Chemistry, 1994 , vol. 59, # 9 p. 2620 - 2622
