2-(羟甲基)丙烯酸甲酯合成路线 (共 28 条)
反应条件
potassium carbonate in water T=20°C; 1 h;
参考文献
Bartrum, Hannah E.; Adams, Harry; Caggiano, Lorenzo; Jackson, Richard F.W.
Tetrahedron, 2008 , vol. 64, # 17 p. 3701 - 3712
反应条件
formaldehyd; paraformaldehyde in diethyl ether; nitrogen
参考文献
Barrera, Jaime Bermejo; Silva, Margarita Hernandez; De Mon, Melchor Alvarez; Ranieri, Juan Pablo Pivel
Patent: US2003/199575 A1, 2003 ;
反应条件
1,4-diaza-bicyclo[2.2.2]octane in 1,4-dioxane; water T=20°C; Baylis-Hillman reaction; 9 h;
参考文献
Guo, Yujuan; Shao, Guang; Li, Lanning; Wu, Wenhao; Li, Ruihong; Li, Jingjing; Song, Jian; Qiu, Liqin; Prashad, Mahavir; Kwong, Fuk Yee
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 9 p. 1539 - 1553
参考文献
BASF Aktiengesellschaft
Patent: US4654432 A1, 1987 ;
反应条件
1,4-diaza-bicyclo[2.2.2]octane T=95°C; 4 h;
参考文献
Synthetic Communications, , vol. 17, # 3 p. 291 - 298
反应条件
potassium carbonate T=20°C; 4 h;
参考文献
Bioscience, Biotechnology, and Biochemistry, , vol. 66, # 7 p. 1501 - 1514
反应条件
1,4-diaza-bicyclo[2.2.2]octane 19 h; Heating;
参考文献
Boffa, Lisa S.; Novak, Bruce M.
Tetrahedron, 1997 , vol. 53, # 45 p. 15367 - 15396
反应条件
methanol; sulfuric acid
参考文献
Journal of the Chemical Society, , p. 236,240
反应条件
(i) AcOH, (ii) /BRN= 506003/, (iii) H2SO4; Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 28, p. 2835 - 2838
反应条件
during storage at low temperature;
参考文献
Drewes, Siegfried E.; Loizou, Georgia; Roos, Gregory H. P.
Synthetic Communications, 1987 , vol. 17, # 3 p. 291 - 298