1-(2,4-二羟基苯基)-2-(4-硝基苯基)-乙酮合成路线 (共 9 条)
反应条件
boron trifluoride diethyl etherate Heating;
参考文献
Xiao, Zhu-Ping; Shi, Da-Hua; Li, Huan-Qiu; Zhang, Li-Na; Xu, Chen; Zhu, Hai-Liang
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 11 p. 3703 - 3710
反应条件
1: zinc(II) chloride; hydrogenchloride / diethyl ether / 20 °C 2: hydrogenchloride; water / |Reflux View Scheme
参考文献
Mascayano, Carolina; Espinosa, Victoria; Sepulveda-Boza, Silvia; Hoobler, Eric K.; Perry, Steve
Chemical Biology and Drug Design, 2013 , vol. 82, # 3 p. 317 - 325
反应条件
1: zinc(II) chloride; hydrogenchloride / diethyl ether / 20 °C 2: hydrogenchloride; water / |Reflux View Scheme
参考文献
Mascayano, Carolina; Espinosa, Victoria; Sepulveda-Boza, Silvia; Hoobler, Eric K.; Perry, Steve
Chemical Biology and Drug Design, 2013 , vol. 82, # 3 p. 317 - 325
反应条件
hydrogenchloride; diethyl ether; zinc(II) chloride durch Erwaermen des Reaktionsprodukts mit Wasser;
参考文献
Dutta; Bose
Journal of Scientific and Industrial Research, 1952 , vol. 11 B, p. 413
反应条件
piperidine; pyridine T=120°C;
参考文献
Dutta; Bose
Journal of Scientific and Industrial Research, 1952 , vol. 11 B, p. 413
反应条件
boron trifluoride diethyl etherate; methanesulfonyl chloride T=100°C; 2 h;
参考文献
Mascayano, Carolina; Espinosa, Victoria; Sepulveda-Boza, Silvia; Hoobler, Eric K.; Perry, Steve
Chemical Biology and Drug Design, 2013 , vol. 82, # 3 p. 317 - 325
反应条件
1: Et3N / 0.17 h / 0 °C 2: mixed anhydride of acetic and formic acid, Et3N / 0.25 h / 80 - 100 °C View Scheme
参考文献
Baker et al.
Journal of the Chemical Society, 1953 , p. 1852,1856
反应条件
in acetic acid 1.) 0 deg C, 2.) 50-55 deg C;
参考文献
Liu; Cheng
Journal of Heterocyclic Chemistry, 1991 , vol. 28, # 6 p. 1641 - 1642
反应条件
1: 1.35 g / morpholine / propan-2-ol / 7 h / 80 °C
2: 30.6 percent / zinc; acetic acid / ethanol / 50 °C
View Scheme
参考文献
Gao, Guang-Yao; Li, Dian-Jun; Keung, Wing Ming
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 18 p. 4069 - 4081