N-甲基-N-苯基苯并三唑甲胺合成路线 (共 9 条)
反应条件
1.) methanol, water, 7 h, 2.) Et2O, reflux, overnight;
参考文献
Katritzky, Alan R.; Yannakopoulou, Konstantina; Lue, Ping; Rasala, Danuta; Urogdi, Laszlo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 225 - 233
反应条件
in diethyl ether 1.) 22 deg C, 2 h, 2.) -5 deg C, 16 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 60, # 8 p. 2588 - 2596
参考文献
Tetrahedron Letters, , vol. 32, # 34 p. 4247 - 4248
反应条件
in toluene 1 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 64, # 2 p. 488 - 492
反应条件
sodium tetrahydroborate in tetrahydrofuran Ambient temperature;
参考文献
Katritzky, Alan R.; Yannakopoulou, Konstantina; Lue, Ping; Rasala, Danuta; Urogdi, Laszlo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 225 - 233
反应条件
gibberellic acid; potassium iodide in tetrahydrofuran T=70°C; 5 h;
参考文献
Bao, Weiliang; Zhang, Yongmin
Synthetic Communications, 1997 , vol. 27, # 4 p. 615 - 620
反应条件
bismuth(III) chloride; aluminium in tetrahydrofuran; water T=20°C;
参考文献
Katritzky, Alan. R.; Shobana, Navayath; Harris, Philip A.
Tetrahedron Letters, 1991 , vol. 32, # 34 p. 4247 - 4248
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=0°C; 2 h;
参考文献
Katritzky, Alan R.; Nichols, Daniel A.; Qi, Ming; Yang, Baozhen
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 4 p. 1259 - 1262
反应条件
in toluene
1 h; Heating;
参考文献
Ahn, Jin Hee; Joung, Meyoung J.; Yoon, Nung Min; Oniciu, Daniela C.; Katritzky, Alan R.
Journal of Organic Chemistry, 1999 , vol. 64, # 2 p. 488 - 492