(1R,2S)-2-苯基环丙胺合成路线 (共 4 条)
反应条件
in methanol 0.166667 h; Irradiation;
参考文献
Journal of the American Chemical Society, , vol. 113, # 24 p. 9251 - 9257
反应条件
in acetonitrile 0.166667 h; Irradiation; Yield given;
参考文献
Journal of the American Chemical Society, , vol. 113, # 24 p. 9251 - 9257
反应条件
1: Heating 2: LiAlH4 / diethyl ether / Heating View Scheme
参考文献
Kaiser,C. et al.
Journal of Organic Chemistry, 1962 , vol. 27, p. 768 - 773
反应条件
2: CH2Cl2 / 0.5 h / Ambient temperature 3: 79 percent / NaH / tetrahydrofuran / 4 h / 70 °C 4: 87 percent / KOH / tetrahydrofuran; H2O / 1.5 h / 65 - 70 °C 5: 90 percent / various solvent(s) / 18 h / 100 - 110 °C 6: 42 percent / 10percent aq. KOH / ethanol / 48 h / Heating View Scheme
参考文献
Mitscher; Sharma; Chu; Shen; Pernet
Journal of Medicinal Chemistry, 1986 , vol. 29, # 10 p. 2044 - 2047