反应条件
1: 69 percent / pyridine, PPh3, Et3N / CCl4; acetonitrile / 24 h
2: 1.) Mg, I2 / 1.) THF, RT, 10 h, 2.) THF, reflux, 5 h
View Scheme
参考文献
Peer, Markus; De Jong, Johannes C.; Kiefer, Matthias; Langer, Thomas; Rieck, Heiko; Schell, Heico; Sennhenn, Peter; Sprinz, Juergen; Steinhagen, Henning; Wiese, Burkhard; Helmchen, Guenter
Tetrahedron, 1996 , vol. 52, # 21 p. 7547 - 7583
