1,3,5-三(2-噻吩基)苯合成路线 （共 12 条）
反应条件
ethylenediamine; trifluoroacetic acid in nitromethane 24 h; Reflux;
参考文献
Zhang, Shao-Liang; Xue, Zhao-Feng; Gao, Ya-Ru; Mao, Shuai; Wang, Yong-Qiang
Tetrahedron Letters, 2012 , vol. 53, # 19 p. 2436 - 2439
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene 12 h; Inert atmosphereReflux;
参考文献
Sumitomo Chemical Company, Limited; Osaka University
Patent: EP2407464 A1, 2012 ;
Location in patent: Page/Page column 24 ;
反应条件
palladium(II) dichloride bis[bis(diphenylphosphine)ferrocene] in tetrahydrofuran; diethyl ether T=20°C; Kumada coupling reaction; 48 h; Inert atmosphereCooling with ice;
参考文献
Cornacchio, Angelica L. P.; Price, Jacquelyn T.; Jennings, Michael C.; McDonald, Robert; Staroverov, Viktor N.; Jones, Nathan D.
Journal of Organic Chemistry, 2009 , vol. 74, # 2 p. 530 - 544
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=50°C; 48 h;
参考文献
Pelter, Andrew; Jenkins, Ieuan; Jones, D. Elfyn
Tetrahedron, 1997 , vol. 53, # 30 p. 10357 - 10400
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; diethyl ether T=60°C; Kumada coupling reaction; Inert atmosphere;
参考文献
Cornacchio, Angelica L. P.; Price, Jacquelyn T.; Jennings, Michael C.; McDonald, Robert; Staroverov, Viktor N.; Jones, Nathan D.
Journal of Organic Chemistry, 2009 , vol. 74, # 2 p. 530 - 544
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in ethanol; water; toluene Suzuki coupling; 48 h; RefluxInert atmosphere;
参考文献
Iannazzo, Laura; Vollhardt, K. Peter C.; Malacria, Max; Aubert, Corinne; Gandon, Vincent
European Journal of Organic Chemistry, 2011 , # 18 p. 3283 - 3292
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in water; toluene T=110°C; Suzuki Coupling; 12 h;
参考文献
Zhang, Shanlin; Jiang, Bo; Zhan, Chuanlang; Huang, Jianhua; Zhang, Xin; Jia, Hui; Tang, Ailing; Chen, Lili; Yao, Jiannian
Chemistry - An Asian Journal, 2013 , vol. 8, # 10 p. 2407 - 2416
反应条件
NSC26899 in acetonitrile T=80°C;
参考文献
Tintillier, P.; Dupas, G.; Bourguignon, J.; Queguiner, G.
Tetrahedron Letters, 1986 , vol. 27, # 21 p. 2357 - 2360
反应条件
[1,2-bis(4-methoxyphenylthio)ethane]cobalt dibromide; zinc(II) iodide; zinc in dichloromethane T=20°C; 0.5 h; Inert atmosphere;
参考文献
Hilt, Gerhard; Hengst, Christoph; Hess, Wilfried
European Journal of Organic Chemistry, 2008 , # 13 p. 2293 - 2297
反应条件
indium(III) chloride; 2-iodophenol in chlorobenzene 24 h; Reflux; regioselective reaction;
参考文献
Xu, Yan-Li; Pan, Ying-Ming; Wu, Qiang; Wang, Heng-Shan; Liu, Pei-Zhen
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8472 - 8476
