2,6-二甲基-3-硝基吡啶合成路线 （共 14 条）
反应条件
1: aq.-ethanolic H2SO4 / elektrochemische Reduktion an einer Kupfer-Kathode 2: aqueous hydrochloric acid / Natriumnitrit hergestellten Diazoniumsalz-Loesung mit Wasser View Scheme
参考文献
Yakugaku Zasshi, , vol. 61, p. 230,232; dtsch. Ref. Nr. 6, S. 91, 94
Chem.Abstr., , p. 2941
反应条件
1: selenium(IV) oxide / 1,4-dioxane / 16 h / 100 °C 2: sodium tetrahydroborate; methanol / 1 h / 0 °C View Scheme
参考文献
Gruenenthal GmbH; FRANK, Robert; BAHRENBERG, Gregor; CHRISTOPH, Thomas; LESCH, Bernhard; LEE, Jeewoo
Patent: US2013/29962 A1, 2013 ;
反应条件
1: 62 percent / ZnCl2, N,N-dimethylformamide / 24 h / 100 °C 2: 1.) ozonized oxygen, 2.) hydrogen peroxide View Scheme
参考文献
Achremowicz, Lucjan
Tetrahedron Letters, 1980 , vol. 21, p. 2433 - 2434
反应条件
1: 61 percent / SeO2, KMnO4
2: 97 percent / decarboxylation
3: 66 percent / 30percent H2O2 / acetic acid; benzene
View Scheme
参考文献
Achremowicz, Lucjan
Tetrahedron Letters, 1980 , vol. 21, p. 2433 - 2434
