(R)-1-叠氮基-4-(甲基亚磺酰)-丁烷合成路线 （共 4 条）
反应条件
in toluene T=0°C; 1 h; Inert atmosphere;
参考文献
Khiar, Noureddine; Werner, Sabine; Mallouk, Siham; Lieder, Franziska; Alcudia, Ana; Fernandez, Inmaculada
Journal of Organic Chemistry, 2009 , vol. 74, # 16 p. 6002 - 6009
反应条件
1: Et3N / CH2Cl2 / 2 h / 0 °C 2: NaN3 / dimethylformamide / 12 h / Ambient temperature View Scheme
参考文献
Whitesell, James K.; Wong, Man-Shing
Journal of Organic Chemistry, 1994 , vol. 59, # 3 p. 597 - 601
反应条件
1: 92 percent / HF / acetonitrile / 0.5 h / Ambient temperature 2: Et3N / CH2Cl2 / 2 h / 0 °C 3: NaN3 / dimethylformamide / 12 h / Ambient temperature View Scheme
参考文献
Whitesell, James K.; Wong, Man-Shing
Journal of Organic Chemistry, 1994 , vol. 59, # 3 p. 597 - 601
反应条件
triphenylphosphine 1.) Et2O, reflux, 3 h, 2.) reflux, 1 h; Yield given. Multistep reaction;
参考文献
Whitesell, James K.; Wong, Man-Shing
Journal of Organic Chemistry, 1994 , vol. 59, # 3 p. 597 - 601
