顺,顺-1,5-环辛二烯合成路线 (共 287 条)
反应条件
Rh(acetylacetonate)-(CO)(PPh3); hydrogen; triphenylphosphine T=80°C; P=7600 Torr; 3 h; Title compound not separated from byproducts;
参考文献
Trzeciak, Anna M.; Ziolkowski, Jozef J.
Journal of Organometallic Chemistry, 1994 , vol. 479, # 1-2 p. 213 - 216
反应条件
hydrogen; rhodium 1.) from -196 deg C to RT, 2.) toluene, 20 deg C, 48 h, 70 atm; Yield given. Multistep reaction;
参考文献
Salvadori, Piero; Vitulli, Giovanni; Raffaelli, Andrea; Lazzaroni, Raffaello
Journal of Organometallic Chemistry, 1983 , vol. 258, # 3 p. 351 - 356
反应条件
sodium hydroxide; sodium tetrahydroborate; dihydrogen peroxide multistep reaction; (per)oxymercuriation of various cyclo-octadienes followed by reduction, influence of mercury(II) salt and reaction conditions; Product distribution;
参考文献
Bloodworth, A.J.; Khan, Jamil A.; Loveitt, M.E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 621 - 632
参考文献
Knights,E.F.; Brown,H.C.
Journal of the American Chemical Society, 1968 , vol. 90, p. 5283 - 5284
参考文献
Knights,E.F.; Brown,H.C.
Journal of the American Chemical Society, 1968 , vol. 90, p. 5283 - 5284
反应条件
in acetonitrile 2 h; UV-irradiation; Further byproducts. Title compound not separated from byproducts.;
参考文献
Yadav, Veejendra K.; Balamurugan, Rengarajan; Parvez, Masood; Yamdagni, Raghav
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 3 p. 323 - 332
反应条件
dibenzoyl peroxide 120 h; Heating;
参考文献
Ashby, E. C.; Coleman, David
Journal of Organic Chemistry, 1987 , vol. 52, # 20 p. 4554 - 4565
反应条件
hydrogen; palladium on activated charcoal in hexane Ambient temperature;
参考文献
Alonso, Francisco; Osante, Inaki; Yus, Miguel
Tetrahedron, 2007 , vol. 63, # 1 p. 93 - 102
反应条件
hydrogen; Pd(II) complex containing tridentate hydrazonic ligands in tetrahydrofuran T=40°C; Hydrogenation; 24 h;
参考文献
Journal of Organometallic Chemistry, , vol. 583, # 1-2 p. 94 - 105
反应条件
zirconocene dichloride; water; diisobutyl-aluminum chloride 1.) 80 deg C, 20 h; Multistep reaction;
参考文献
Dzhemilev, U. M.; Ibragimov, A. G.; Vostrikova, O. S.; Vasil'eva, E. V.; Tolstikov, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, p. 1004 - 1009
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , vol. 36, # 5 p. 1089 - 1095