顺,顺-1,5-环辛二烯合成路线 (共 287 条)
反应条件
1: 20 h / 100 °C / Inert atmosphere; Neat (no solvent) 2: 3,4-dihydroxy-1-tert-butylbenzene; oxygen / 1,2-dichloro-ethane / 3 h / 80 °C View Scheme
参考文献
Villa, Giorgio; Povie, Guillaume; Renaud, Philippe
Journal of the American Chemical Society, 2011 , vol. 133, # 15 p. 5913 - 5920
反应条件
nickel in nitrogen; N,N-dimethyl-formamide; toluene; aluminium
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: US2011/95269 A1, 2011 ;
反应条件
copper acetylacetonate in chloroform 1.25 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2839 - 2846
反应条件
carbon monoxide; hydrogen; sodium acetate; copper dichloride; palladium dichloride; palladium on activated charcoal 1.) methanol, RT, 24 h, 417 kPa; Multistep reaction;
参考文献
Anderson, Curtis B.; Markovic, Rade
Collection of Czechoslovak Chemical Communications, 1991 , vol. 56, # 3 p. 663 - 672
反应条件
carbon monoxide; hydrogen; sodium acetate; copper dichloride; palladium dichloride; palladium on activated charcoal 1.) RT, 24 h, 417 kPa; Multistep reaction;
参考文献
Anderson, Curtis B.; Markovic, Rade
Collection of Czechoslovak Chemical Communications, 1991 , vol. 56, # 3 p. 663 - 672
反应条件
hydrogen; sodium acetate; copper dichloride; palladium dichloride; palladium on activated charcoal 1.) RT, 24 h, 417 kPa; Multistep reaction;
参考文献
Anderson, Curtis B.; Markovic, Rade
Collection of Czechoslovak Chemical Communications, 1991 , vol. 56, # 3 p. 663 - 672
反应条件
dipotassium hydrogenphosphate; 3-chloro-benzenecarboperoxoic acid in dichloromethane; water T=0 - 20°C;
参考文献
Akbulatov, Sergey; Tian, Yancong; Boulatov, Roman
Journal of the American Chemical Society, 2012 , vol. 134, # 18 p. 7620 - 7623
反应条件
phosphoric acid; sulfuric acid; dihydrogen peroxide; sodium tungstate; Aliquatreg; 336 in water; 1,2-dichloro-ethane T=70°C; pH=1.6; 1 h; microwave irradiation;
参考文献
Bogdal; Lukasiewicz; Pielichowski; Bednarz
Synthetic Communications, 2005 , vol. 35, # 23 p. 2973 - 2983
反应条件
oxygen; isobutyraldehyde in acetonitrile T=60°C; 4 h;
参考文献
Pielichowski, Jan; Kowalski, Grzegorz
Molecular Crystals and Liquid Crystals, 2010 , vol. 522, p. 105 - 111
反应条件
oxygen T=90°C; 3.5 h; var. reaction procedures, also in the presence of initiator and inhibitor of free-radical reaction; Product distributionMechanism;
参考文献
Giezynski, Roman; Pala, Magdalena
Polish Journal of Chemistry, 1986 , vol. 60, # 1-3 p. 85 - 90