顺,顺-1,5-环辛二烯合成路线 (共 287 条)
反应条件
ozone in dichloromethane T=-78°C;
参考文献
European Journal of Organic Chemistry, , # 16 p. 3083 - 3087
反应条件
ozone in dichloromethane T=-78°C;
参考文献
European Journal of Organic Chemistry, , # 16 p. 3083 - 3087
反应条件
Yield given. Multistep reaction;
参考文献
Odinokov; Botsman; Gladysheva
Chemistry of Natural Compounds, 1996 , vol. 32, # 3 p. 381 - 383
反应条件
1: 55 g / Me4Sn / MoCl5/SiO2 / toluene / 24 h / 20 °C 2: 90 percent / LiAlH4; Cp2ZrCl2 / tetrahydrofuran / 1 h / 20 °C 3: 92 percent / 9-BBN; NaOH; H2O2 / tetrahydrofuran; methanol 4: 93 percent / pyridine / hexane / 2 h / 12 - 20 °C View Scheme
参考文献
Bykov; Butenko; Egupova; Finkelshtein
Russian Chemical Bulletin, 2000 , vol. 49, # 7 p. 1301 - 1304
反应条件
3-chloro-benzenecarboperoxoic acid in tetrahydrofuran; chloroform T=20°C; 18 h;
参考文献
Allcock, Harry R.; Welna, Daniel T.; Stone, David A.
Macromolecules, 2005 , vol. 38, # 25 p. 10406 - 10412
反应条件
dipotassium hydrogenphosphate; 3-chloro-benzenecarboperoxoic acid in dichloromethane; water T=0 - 20°C;
参考文献
Akbulatov, Sergey; Tian, Yancong; Boulatov, Roman
Journal of the American Chemical Society, 2012 , vol. 134, # 18 p. 7620 - 7623
反应条件
pyridine; dihydrogen peroxide; methyltrioxorhenium (VII) in dichloromethane 5 h; Ambient temperature;
参考文献
Rudolph; Reddy; Chiang; Sharpless
Journal of the American Chemical Society, 1997 , vol. 119, # 26 p. 6189 - 6190
反应条件
pyridine-2,6-dicarboxylic acid; FeCl3·6H2O; N1,N1-Dimethyl-N2-cyclohexylformamidine; dihydrogen peroxide in 1,1-dimethylpropan-1-ol; water T=20°C; 1 h; Air; chemoselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 352, # 10 p. 1771 - 1778
反应条件
dihydrogen peroxide; WO3 mesoporous catalyst in tert-butyl alcohol T=60°C; 24 h; Product distribution; Further Variations:Catalysts;
参考文献
Gao, Ruihua; Yang, Xinli; Dai, Wei-Lin; Le, Yingyi; Li, Hexing; Fan, Kangnian
Journal of Catalysis, 2008 , vol. 256, # 2 p. 259 - 267
反应条件
oxygen T=80°C; P=759.8 Torr; 25 h; Mechanism;
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 322, # 6 p. 915 - 932