顺,顺-1,5-环辛二烯合成路线 (共 287 条)
参考文献
Joy,F. et al.
Journal of Organometallic Chemistry, 1966 , vol. 5, p. 506 - 519
反应条件
Rh(acetylacetonate)-(CO)(PPh3); hydrogen; triphenylphosphine T=80°C; P=7600 Torr; 3 h; Title compound not separated from byproducts;
参考文献
Journal of Organometallic Chemistry, , vol. 479, # 1-2 p. 213 - 216
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bestmann, Hans Juergen; Roeder, Thomas; Suehs, Kurt
Chemische Berichte, 1988 , vol. 121, p. 1509 - 1518
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chemische Berichte, , vol. 121, p. 1509 - 1518
反应条件
hydroquinone in ethanol; water was prepared by modification of method described in (Benzman et al. Inorg. Chem. 19 (1980) 3755). heating of H2IrCl6*xH2O and hydroquinone in EtOH-water (2:1) at reflux for 1 h under N2, addn. of C8H12, reflux for 4 h; concn., addn. of water, cooling to room temp., filtration, washing with cold CH3OH, drying in vac. over P2O5;
参考文献
Inorganica Chimica Acta, , vol. 359, # 12 p. 3800 - 3806
反应条件
tetramethylstannane; [MoCl5]; silica gel in toluene T=20°C; P=9120 Torr; 48 h;
参考文献
Bykov; Goletiani; Butenko; Finkelshtein
Russian Chemical Bulletin, 2004 , vol. 53, # 11 p. 2650 - 2652
反应条件
1: aq. HCl / Pd(acac)2 2: (i) NaMnO4, (ii) SO2, (iii) /BRN= 1718733/, benzene 3: NaH / benzene / Heating 4: aq. HCl, AcOH / Heating View Scheme
参考文献
Tsuji,J. et al.
Bulletin of the Chemical Society of Japan, 1966 , vol. 39, p. 141 - 145
反应条件
pyridinium tribromide in methanol
参考文献
Eglinton,G. et al.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 474 - 479
反应条件
tetrachloromethane; bromine
参考文献
Detert, Heiner; Rose, Bernd; Mayer, Winfried; Meier, Herbert
Chemische Berichte, 1994 , vol. 127, # 8 p. 1529 - 1532