(2S)-3,3-二甲基-2'H-螺[双环[2.2.1]庚烷-2,4'-[1,3]恶唑烷]-2'-酮合成路线 （共 3 条）
反应条件
in 1,1,2,2-tetrachloroethylene
参考文献
Banks, Malcolm R.; Blake, Alexander J.; Brown, Angus R.; Cadogan, J. I. G.; Gaur, Suneel; et al.
Tetrahedron Letters, 1994 , vol. 35, # 3 p. 489 - 492
反应条件
1: Et3N / toluene; diethyl ether / 0 °C 2: sodium azide, Bu4NBr / CH2Cl2; H2O / 25 °C 3: 70 percent / tetrachloroethene View Scheme
参考文献
Banks, Malcolm R.; Blake, Alexander J.; Brown, Angus R.; Cadogan, J. I. G.; Gaur, Suneel; et al.
Tetrahedron Letters, 1994 , vol. 35, # 3 p. 489 - 492
反应条件
1: 1.) BH3, 2.) KOH, H2O2 / 1.) THF 2: 95 percent / NEt3 3: 95 percent / NaN3, PTC 4: various solvent(s) / 147 °C View Scheme
参考文献
Banks, Malcolm R.; Cadogan, J. I. G.; Gosney, Ian; Grant, Keith J.; Hodgson, Philip K. G.; Thorburn, Paul
Heterocycles, 1994 , vol. 37, # 1 p. 199 - 206
