3-(2-甲基-2-丙基)-7-氧杂双环[4.1.0]庚烷合成路线 （共 4 条）
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane T=20°C; 1 h;
参考文献
Cambie, Richard C.; Chambers, David; Lindsay, Barry G.; Rutledge, Peter S.; Woodgate, Paul D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 822 - 827
反应条件
1: 75 percent / KOMe, 18-crown-6 / tetrahydrofuran 2: 61 percent / K2CO3 / aq. ethanol / 48 h 3: pyridine / diethyl ether / 0 °C 4: 87 percent / 82percent m-chloroperoxybenzoic acid / CH2Cl2 / 16 h / 0 °C View Scheme
参考文献
Lambert,J.B.; Wang,G.; Finzel,R.B.
Journal of the American Chemical Society, 1987 , vol. 109, p. 7838
反应条件
1: 61 percent / K2CO3 / aq. ethanol / 48 h 2: pyridine / diethyl ether / 0 °C 3: 87 percent / 82percent m-chloroperoxybenzoic acid / CH2Cl2 / 16 h / 0 °C View Scheme
参考文献
Lambert,J.B.; Wang,G.; Finzel,R.B.
Journal of the American Chemical Society, 1987 , vol. 109, p. 7838
反应条件
1: pyridine / diethyl ether / 0 °C 2: 87 percent / 82percent m-chloroperoxybenzoic acid / CH2Cl2 / 16 h / 0 °C View Scheme
参考文献
Lambert,J.B.; Wang,G.; Finzel,R.B.
Journal of the American Chemical Society, 1987 , vol. 109, p. 7838
