4,7-二甲基-1H-吲哚-2,3-二酮合成路线 （共 13 条）
反应条件
sulfuric acid in water T=60 - 75°C; 0.916667 h;
参考文献
Guise, G. Bruce; Ollis, W. David; Peacock, Judith A.; Stephanatou, Julia Stephanidou; Stoddart, J. Fraser
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 8 p. 1637 - 1648
反应条件
1: Na2SO4, conc. HCl, hydroxylamine hydrochloride / H2O / 1.5 h / Heating 2: 96percent sulfuric acid / H2O / 1 h / 80 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 106, # 23 p. 7195 - 7200
反应条件
triphenyl-phosphine oxide in xylene Rearrangement; hydrolysis; oxidation; 3 h; Heating;
参考文献
Tetrahedron, , vol. 56, # 11 p. 1551 - 1560
反应条件
4-(N,N-dimethlyamino)pyridine in xylene Rearrangement; hydrolysis; oxidation; 5 h; Heating;
参考文献
Tetrahedron, , vol. 56, # 11 p. 1551 - 1560
反应条件
4-(N,N-dimethlyamino)pyridine in xylene Rearrangement; hydrolysis; oxidation; 5 h; Heating;
参考文献
Tetrahedron, , vol. 56, # 11 p. 1551 - 1560
反应条件
1: 86 percent / AcOOH 2: 1 percent / Ph3PO / xylene / 3 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 56, # 11 p. 1551 - 1560
反应条件
nitrobenzene anschliessend Erwaermen mit Aluminiumchlorid;
参考文献
DE514595 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 17, p. 646
反应条件
1: hydrogenchloride; sodium hydroxide; dihydrogen peroxide / water / 70 °C / pH Ca. 4 2: ethanol; ethyl acetate; diethyl ether / 1.5 h / 20 °C / |Cooling with ice View Scheme
参考文献
SUMITOMO CHEMICAL COMPANY, LIMITED; YOSHIMOTO, Yuya; ARIMORI, Sadayuki; MATSUZAKI, Yuichi
Patent: WO2013/162072 A1, 2013 ;
反应条件
dihydrogen peroxide; sodium methylate 1.) 0-10 deg C 2.) room temperature, 30 min; Yield given. Multistep reaction;
参考文献
Reissenweber, Gernot; Mangold, Dietrich
Angewandte Chemie, 1981 , vol. 93, # 10 p. 914 - 915
反应条件
sodium hydroxide; dihydrogen peroxide T=85 - 90°C;
参考文献
Guise, G. Bruce; Ollis, W. David; Peacock, Judith A.; Stephanatou, Julia Stephanidou; Stoddart, J. Fraser
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 8 p. 1637 - 1648
