sodium hydroxide; dihydrogen peroxide T=85 - 90°C;

potassium hydroxide; Ca(OCl)2; potassium carbonate in water T=50°C; 0.5 h;

1: 96percent sulfuric acid / H2O / 1 h / 80 °C 2: 183.5 g / NaOH, 30percent H2O2 / H2O View Scheme

1: Na2SO4, conc. HCl, hydroxylamine hydrochloride / H2O / 1.5 h / Heating 2: 96percent sulfuric acid / H2O / 1 h / 80 °C 3: 183.5 g / NaOH, 30percent H2O2 / H2O View Scheme

dihydrogen peroxide; sodium methylate 1.) 0-10 deg C 2.) room temperature, 30 min; Yield given. Multistep reaction;

1: isoamyl nitrite / 1,2-dichloro-ethane; bis-(2-methoxy-ethyl) ether / 2 h / Heating 2: H2 / 10percent Pd/C / ethanol / 0 °C 3: 1.) O3/O2, 2.) H2 / 2.) Pd/BaSO4 / 1.) EtOAc, -78 deg C, 7 min, 2.) EtOAc, 0 deg C 4: 52 percent / piperidine, CH3COOH / benzene / 0.5 h / Heating 5: 700 °C / 0.04 Torr / other temperatures, other products on flash vacuum pyrolysis View Scheme

in diethyl ether; ethanol; ethyl acetate T=20°C; 1.5 h; Cooling with ice;

暂无反应条件数据

isopentyl nitrite in tetrahydrofuran; 1,2-dichloro-ethane 3 h; Reflux;

sulfuric acid bei der elektrolytischen Reduktion an Bleikathoden;