反应条件
1: NaH / tetrahydrofuran / 4.5 h / 20 °C
2: 1.) LDA / 1.) THF, -60 deg C, 2 h, 2.) THF, 1 h
3: 33 percent / CH2Cl2 / 24 h / 20 °C
4: 76 percent / AlCl3 / CH2Cl2 / 0.17 h / 20 °C
5: 78 percent / KF, KHCO3, 30percent H2O2/H2O / tetrahydrofuran; methanol / 17 h / 20 °C
6: 70 percent / O2 / Irradiation
View Scheme
参考文献
Krohn, Karsten; Khanbabaee, Karamali
Angewandte Chemie, 1994 , vol. 106, # 1 p. 100 - 102
