2-氨基-4-苄氧基-5-甲氧基苯甲酸合成路线 （共 8 条）
反应条件
tin(ll) chloride in methanol T=70°C; 5 h;
参考文献
Hu; Wang; Lin; Hsu
Journal of Organic Chemistry, 2001 , vol. 66, # 8 p. 2881 - 2883
反应条件
boron trifluoride diethyl etherate; sodium iodide in acetonitrile T=20°C; 0.583333 h;
参考文献
Kamal, Ahmed; Shankaraiah; Markandeya; Reddy, Ch. Sanjeeva
Synlett, 2008 , # 9 p. 1297 - 1300
反应条件
sodium hydroxide in methanol 1 h; Heating;
参考文献
Wang, Tiansheng; Lui, Alfred S.; Cloudsdale, Ian S.
Organic Letters, 1999 , vol. 1, # 11 p. 1835 - 1837
反应条件
1: 95.8 percent / sodium borohydride / nickel(II) chloride hexahydrate / methanol; CH2Cl2 / 0.5 h / 0 - 5 °C 2: 98 percent / aq. sodium hydroxide / methanol / 1 h / Heating View Scheme
参考文献
Organic Letters, , vol. 1, # 11 p. 1835 - 1837
反应条件
1: 58.6 percent / potassium carbonate / acetone / 3 h / Heating 2: 82.6 percent / nitric acid / tin(IV) chloride / CH2Cl2 / 0.17 h / -20 °C 3: 95.8 percent / sodium borohydride / nickel(II) chloride hexahydrate / methanol; CH2Cl2 / 0.5 h / 0 - 5 °C 4: 98 percent / aq. sodium hydroxide / methanol / 1 h / Heating View Scheme
参考文献
Organic Letters, , vol. 1, # 11 p. 1835 - 1837
反应条件
1: 82.6 percent / nitric acid / tin(IV) chloride / CH2Cl2 / 0.17 h / -20 °C 2: 95.8 percent / sodium borohydride / nickel(II) chloride hexahydrate / methanol; CH2Cl2 / 0.5 h / 0 - 5 °C 3: 98 percent / aq. sodium hydroxide / methanol / 1 h / Heating View Scheme
参考文献
Organic Letters, , vol. 1, # 11 p. 1835 - 1837
反应条件
in methanol; ethyl acetate
参考文献
Kaohsiung Medical University
Patent: US2003/187253 A1, 2003 ;
反应条件
sodium azide; sulfuric acid; sodium nitrite in water 12 h; Ambient temperature;
参考文献
Eguchi, Shoji; Yamashita, Keizo; Matsushita, Yuji; Kakehi, Akikazu
Journal of Organic Chemistry, 1995 , vol. 60, # 13 p. 4006 - 4012
