反应条件
1: 1) LiH / 1) acetonitrile, 40 degC, 2 h, 2) room temp., 24 h
2: 82 percent / HOAc / 60 °C
3: 83.4 percent / H2 / Pd/C (10percent) / ethanol; acetic acid / 1 h
4: 63 percent / SO2Cl2 / acetonitrile / 1.5 h / 35 - 40 °C
5: 62 percent / HOAc / CH2Cl2 / 0.17 h / Ambient temperature
View Scheme
参考文献
Bouillon, Guenther; Schank, Kurt
Chemische Berichte, 1980 , vol. 113, # 8 p. 2630 - 2635
