氘代3-氨基-5-吗啉-4-甲基-恶唑-2-啉酮合成路线 （共 36 条）
反应条件
in tetrahydrofuran; pentane byproducts: LiCl; (N2), added at 0°C, stirred for 2 h at 0°C, stirred for 5 h at 20°C; filtered, solvent removed in vacuo, fractionated distillation, elem. anal.;
参考文献
Chemische Berichte, , vol. 124, p. 1497 - 1504
反应条件
in benzene byproducts: LiCl; under N2 or Ar or in vac., reflux for 4 h; cooled to room temp., filtered, washed with hexane; elem. anal.;
参考文献
Koelle, Peter; Linti, Gerald; Noeth, Heinrich; Wood, Gary L.; Narula, Chaitanya K.; Paine, Robert T.
Chemische Berichte, 1988 , vol. 121, p. 871 - 880
反应条件
in pentamethylene under N2, addn. of Re-compound in 5 portions at 0°C, stirred at 20.degrree.C overnight; removal of volatiles in vac., dissolved in n-pentane, filtration, washed with n-pentane, fractd. crystn. at -28°C (filtrate); elem. anal.;
参考文献
Weber, Lothar; Meine, Georg; Boese, Roland; Blaeser, Dieter
Chemische Berichte, 1988 , vol. 121, p. 853 - 858
反应条件
phosphorus trichoride
参考文献
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, , vol. 35, # 5 p. 594 - 598
反应条件
in toluene reaction of the Pt complex with 2 equiv. LiP(SiMe3)2 at low temps.; mixt. warmed to room temp.; products not isolated, detected by (31)P-NMR;
参考文献
Zeitschrift fuer Anorganische und Allgemeine Chemie, , vol. 560, p. 65 - 79
反应条件
in toluene under protective gas; 8.8 mmol of the Li salt in toluene added to 4 mmol of the Pt complex in toluene at -20°C; mixt. warmed to 20°C and stirred for 2 d; filtration; filtrate evapd. in vac.; fractionated crystn.;
参考文献
Zeitschrift fuer Anorganische und Allgemeine Chemie, , vol. 560, p. 65 - 79
反应条件
in toluene under protective gas; reaction of equimolar amts. of the Li salt and the Pt complex in toluene at low temps.; mixt. then warmed up to room temp.; products not isolated (except (PPh3)3Pt), detected by (31)P-NMR;
参考文献
Zeitschrift fuer Anorganische und Allgemeine Chemie, , vol. 560, p. 65 - 79
参考文献
Bruker,A.B. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1966 , vol. 36, p. 75 - 78,79 - 81
参考文献
Gmelin Handbook: F: PerFHalOrg.SVol.1, 5.2.2, page 81 - 87
反应条件
zinc(II) chloride T=80°C; 2 h;
参考文献
Prishchenko, A.A.; Livantsov, M.V.; Petrosyan, V.S.
Russian Journal of General Chemistry, 1994 , vol. 64, # 8.2 p. 1181 - 1193
Zhurnal Obshchei Khimii, 1994 , vol. 64, # 8 p. 1316 - 1330
