氘代3-氨基-5-吗啉-4-甲基-恶唑-2-啉酮合成路线 （共 36 条）
参考文献
Povolotskii, M. I.; Negrebetskii, V. V.; Romanenko, V. D.; Ivanchenko, V. I.; Sarina, T. V.; Markovskii, L. N.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 10.1 p. 2238 - 2244,2000 - 2005
反应条件
3 w, molar ratio of ((CH3)3Si)3P to CF3AsH2 2:8.5;
参考文献
Ansari, S.; Grobe, J.
Z. Naturforsch. b, 1975 , vol. 30, p. 523 - 530
反应条件
in dichloromethane
1 h; RefluxInert atmosphere;
参考文献
Prishchenko, Andrey A.; Livantsov, Mikhail V.; Novikova, Olga P.; Livantsova, Ludmila I.; Petrosyan, Valery S.
Heteroatom Chemistry, 2010 , vol. 21, # 6 p. 441 - 445
反应条件
in tetrahydrofuran
protective gas, room temp., 12 h; molar product ratio ((DPPE)Ni)2P2 : (DPPE)2Ni = 1:4 (by (31)P-NMR-spectroscopy);
参考文献
Schaefer, H.; Binder, D.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1988 , vol. 557, p. 45 - 58
反应条件
in tetrahydrofuran
under Ar, 12 h at room temp.; isolation by fractd. crystn. not complete, molar product ratio ((DEPE)Ni)2P2 : (DEPE)2Ni = 2:3;
参考文献
Schaefer, H.; Binder, D.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1988 , vol. 557, p. 45 - 58
反应条件
in tetrahydrofuran
under Ar, room temp., 14 d; molar product ratio ((DCPE)Ni)2P2 : (DCPE)2Ni = 1:1;
参考文献
Schaefer, H.; Binder, D.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1988 , vol. 557, p. 45 - 58
