zinc(II) tetrahydroborate; silica gel in ethylene glycol dimethyl ether 6 h; Ambient temperature;

tert.-butylhydroperoxide; copper(l) iodide in water 24 h; Reflux;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1209320', constants.ctx, '0')">sodium azide</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '635680', constants.ctx, '0')">acetone</a> <br />T=20&deg;C;&nbsp;<br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '11343689', constants.ctx, '0')">dipotassium peroxodisulfate</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '1216827', constants.ctx, '0')">2,4,6-trimethylbenzene-1-sulfonyl azide</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '3659919', constants.ctx, '0')">silver fluoride</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '741857', constants.ctx, '0')">acetonitrile</a> <br />T=55&deg;C;&nbsp;P=760.051&nbsp;Torr;&nbsp;48&nbsp;h;&nbsp;&nbsp;Inert atmosphereSchlenk technique;&nbsp;<br /> &nbsp;