3-苄基-3-氮杂双环[3.1.0]-6-己胺合成路线 （共 4 条）
反应条件
hydrazine in methanol; water T=20°C; 5 h;
参考文献
SUNSHINE LAKE PHARMA CO., LTD.; ZHANG, Jiancun; ZHANG, Yingjun; ZHANG, Weihong; LIU, Bing; ZHANG, Jiquan; LIU, Jinlei; ZHANG, Lu
Patent: WO2013/71697 A1, 2013 ;
Location in patent: Paragraph 00353 ;
反应条件
1: borane-THF / tetrahydrofuran / 1 h / |Reflux 2: hydrazine / methanol; water / 5 h / 20 °C View Scheme
参考文献
SUNSHINE LAKE PHARMA CO., LTD.; ZHANG, Jiancun; ZHANG, Yingjun; ZHANG, Weihong; LIU, Bing; ZHANG, Jiquan; LIU, Jinlei; ZHANG, Lu
Patent: WO2013/71697 A1, 2013 ;
反应条件
1: potassium carbonate / acetonitrile / 24 h / 20 °C 2: borane-THF / tetrahydrofuran / 1 h / |Reflux 3: hydrazine / methanol; water / 5 h / 20 °C View Scheme
参考文献
SUNSHINE LAKE PHARMA CO., LTD.; ZHANG, Jiancun; ZHANG, Yingjun; ZHANG, Weihong; LIU, Bing; ZHANG, Jiquan; LIU, Jinlei; ZHANG, Lu
Patent: WO2013/71697 A1, 2013 ;
反应条件
triethylamine in dichloromethane T=0 - 20°C; 4 h;
参考文献
RANBAXY LABORATORIES LIMITED
Patent: WO2006/56863 A1, 2006 ;
Location in patent: Page/Page column 37-38 ;
