5,9,14,18,23,27,32,36-八丁氧基-2,3-萘酞菁铜(II)合成路线 (共 1 条)
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in butan-1-ol under Ar atm. mixt. Co(OAc)2*4H2O, naphthalocyanine, 1,8-diazabicyclo(5.4.0)undec-7-ene and 1-butanol was refluxed for 20 h; react. mixt. was diluted with MeOH and H2O, ppt. was filtered and chromed. on Al2O3-V (toluene), vac.-dried at room temp.;
参考文献
Soldatova, Alexandra V.; Kim, Junhwan; Rosa, Angela; Ricciardi, Giampaolo; Kenney, Malcolm E.; Rodgers, Michael A. J.
Inorganic Chemistry, 2008 , vol. 47, # 10 p. 4275 - 4289