(氯甲基)甲基-二氯硅烷合成路线 （共 42 条）
反应条件
in pentane 1) 0 deg C, 3 h 2) 23 deg C, 7 h;
参考文献
Bienz, Stefan; Chapeaurouge, Alexander
Helvetica Chimica Acta, 1991 , vol. 74, # 7 p. 1477 - 1488
反应条件
aluminium trichloride
参考文献
Tschernyschew et al.
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 2676,2680; engl.Ausg.S.2718,2722
反应条件
1H-imidazole; 4-(N,N-dimethlyamino)pyridine in dichloromethane T=0 - 20°C; 12 h; Inert atmosphereSchlenk technique;
参考文献
Erhardt, Sascha A.; Hoffmann, Florian; Daiss, Juergen O.; Stohrer, Juergen; Herdtweck, Eberhardt; Rieger, Bernhard
Chemistry - A European Journal, 2013 , vol. 19, # 15 p. 4818 - 4825
反应条件
1.) ether, reflux, 4h; 2.) ether, reflux, 4 h; Yield given. Multistep reaction;
参考文献
Terunuma, Daiyo; Kato, Masato; Kamei, Masanao; Uchida, Hidekatsuu; Ueno, Satoshi; Nohira, Hiroyuki
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, p. 3581 - 3588
参考文献
Lambertsen, Thomas; Schmutzler, Reinhard
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1995 , vol. 50, # 11 p. 1583 - 1586
反应条件
magnesium
1) Et2O, 2a) pettrol ether, 14h, RT, 2b) 8h, reflux; Yield given. Multistep reaction;
参考文献
Tacke, Reinhold; Wiesenberger, Frank; Becker, Beate; Rohr-Aehle, Regine; Schneider, Petra B.; et al.
Chemische Berichte, 1992 , vol. 125, # 3 p. 591 - 606
反应条件
oxygen in benzene
byproducts: Et3GeCl, (Et3Ge)2O; mixing the compds. in benzene in an evacuated glass ampul, opening the ampul to the air, occasional shaking (12 h); separating from metallic Hg, vac. distn.; identification by gas-liqiud chromy.;
参考文献
Rybin, L. I.; Gendin, D. V.; Vyazankina, O. A.; Vyazankin, N. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, p. 2216 - 2217
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , p. 2392 - 2393
反应条件
in benzene
byproducts: Et3GeCl; Irradiation (UV/VIS); Ge-compd. addn. to Si-compd. soln., sealing in evac. ampul, irradiation (DRT-375 quartz mercury lamp) until orange color of Ge-compd. disappeared (3 min); fractionation; elem. anal.;
参考文献
Gendin, D. V.; Rybin, L. I.; Vyazankina, O. A.; Vyazankin, N. S.
Journal of General Chemistry USSR (English Translation), 1983 , vol. 53, p. 1293 - 1294
Zhurnal Obshchei Khimii, 1983 , vol. 53, p. 1438 - 1439
反应条件
byproducts: Et3SiCl; Irradiation (UV/VIS); irradiated for 3 min; distd.; GLC; elem. anal.;
参考文献
Gendin, D. V.; Rybin, L. I.; Larin, M. F.; Vyazankina, O. A.; Vyazankin, N. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, p. 1930 - 1931
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , vol. 32, p. 2137 - 2138
参考文献
D'yakov,V.M. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1978 , vol. 27, # 10 p. 2098 - 2104
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1978 , vol. 27, # 10 p. 2366 - 2372
