3-苯胺基-3-羰基丙酸合成路线 (共 24 条)
反应条件
lithium hydroxide; water in tetrahydrofuran; methanol T=20°C; 3 h;
参考文献
Dolle, Roland E.; Chu, Guo-Hua; Gu, Minghua
Patent: US2005/107355 A1, 2005 ;
Location in patent: Page/Page column 34 ;
反应条件
5 Pd/C; hydrogen in methanol T=20°C; P=760.051 Torr; 16 h;
参考文献
Sechi, Mario; Azzena, Ugo; Delussu, Maria Paola; Dallocchio, Roberto; Dessi, Alessandro; Cosseddu, Alessia; Pala, Nicolino; Neamati, Nouri
Molecules, 2008 , vol. 13, # 10 p. 2442 - 2461
反应条件
in tetrahydrofuran; dichloromethane T=60°C; 9 h;
参考文献
Im, Isak; Lee, Eui Seung; Choi, Soo Jeong; Lee, Ju-Yeon; Kim, Yong-Chul
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 13 p. 3632 - 3636
反应条件
1: CH2Cl2 / 24 h / Ambient temperature 2: LiOH / methanol; H2O / 15 h View Scheme
参考文献
Anandan, Sampath-Kumar; Ward, John S.; Brokx, Richard D.; Bray, Mark R.; Patel, Dinesh V.; Xiao, Xiao-Xi
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 8 p. 1969 - 1972
反应条件
ethanol; water; sodium carbonate
参考文献
Chattaway; Olmsted
Journal of the Chemical Society, 1910 , vol. 97, p. 939
参考文献
Dieckmann; Hoppe; Stein
Chemische Berichte, 1904 , vol. 37, p. 4633
Full Text Show Details
Michael
Chemische Berichte, 1905 , vol. 38, p. 33
反应条件
sodium; toluene anschliessend Behandeln mit CO2;
参考文献
Nation.Distillers Prod.Corp.
Patent: US2782231 , 1952 ;
反应条件
hydrogenchloride; sodium hydroxide 1.) 156 deg C; 2.) reflux, 1 h; Yield given. Multistep reaction;
参考文献
Paull, Keneth D.; Shoemaker, Robert H.; Boyd, Michael R.; Parsons, Jack L.; Risbood, Prabhakar A.; et al.
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 911 - 914
反应条件
1: alkali 2: methanolic KOH-solution View Scheme
参考文献
Dieckmann; Hoppe; Stein
Chemische Berichte, 1904 , vol. 37, p. 4633
反应条件
in diethyl ether Heating;
参考文献
Douglas, Kenneth T.; Alborz, Manoochehr; Rullo, Gregory R.; Yaggi, Norbert F.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 1675 - 1680